Hielscher Ultrasonics
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Superior Nano-Fuels by Ultrasonic Dispersion

Nanofuel development starts with effective dispersion. Nanoparticles added to diesel, biodiesel, or blended fuels can influence combustion, but their performance depends on how well they are distributed throughout the liquid. Agglomeration and sedimentation make it harder to maintain a consistent additive concentration and obtain reproducible results. Ultrasonic dispersion addresses this challenge by breaking up particle clusters and distributing nano-additives throughout the fuel.

Nano-Fuels

Nanofuels consist in a mixture of a base fuel (e.g. diesel, biodiesel, fuel blends) and nano-particles. Those nanoparticles act as hybrid nanocatalysts, which offer a large reactive surface area. The ultrasonic dispersion of the nano-additive results in substantially improves fuel performance such as reduced ignition delay, longer flame sustenance and agglomerate ignition as well as significant overall reductions in the emission.
Nano-sized fuel-particle blends excel pure liquid fuel regarding fuel performance by higher energy density, faster and easier ignition, enhanced catalytic effect, reduced emission, faster evaporation and burning rate and improved combustion efficiency.
Use sonication for nano-dispersing particles in fuels!

Develop your next Nanofuel Formulation with Sonication!
Contact our team to explore ultrasonic dispersion for your fuel and nanoparticle combination.

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Inline processing with 7kW power ultrasonic processors (Click to enlarge!)

7kW ultrasonic flow system

Nanofuels: Ultrasonic Dispersion of Nanoparticles in Fuel

To avoid the settling of nanoparticles in the fuel tank, the particles must be dispersed sophistically. Ultrasonic dispersion helps incorporate nanoparticles such as cerium oxide, aluminum oxide, and carbon nanotubes into diesel, biodiesel, and fuel blends.
Through acoustic cavitation – the formation and collapse of microscopic bubbles – sonication generates intense local shear forces that break apart particle agglomerates and distribute the additives throughout the liquid. This exposes more particle surface to the surrounding fuel, supporting the evaluation of catalytic and combustion-related benefits.
Ultrasound delivers its dispersing action directly into the liquid without added milling beads, eliminating the need to separate grinding media afterward. Hielscher sonicators support both batch preparation and continuous inline processing, making the technique useful from laboratory research through industrial production.

The list below gives you an overview over already tested nano-materials dispersed in fuels:

  • CNTs – carbon nanotubes
  • Ag – silver
  • Al – aluminium
  • Al2O3 – aluminum oxide
  • AlCuOx – aluminum copper oxides
  • B – boron
  • Ca – calcium
  • CaCO3 – calcium carbonate
  • Fe – iron
  • Cu – copper
  • CuO – copper oxide
  • Ce – cerium
  • CeO2 – cerium oxide
  • (CeO2)·(ZrO2) – cerium zirconium oxide
  • Co – cobalt
  • Mg – magnesium
  • Mn – manganese
  • TiO2 – titanium dioxide
  • ZnO – zinc oxide
Ultrasonic Nano-Dispersion - Sonicator UP400StObserve how the Hielscher UP400St sonicator converts carbon powder and water into a stable nano-dispersion. Intense ultrasound waves and acoustic cavitation achieve rapid particle size reduction, uniform deagglomeration, and highly reproducible results. In contrast to other lab dispersers, Hielscher sonicators allow for linear scale-up enabling a seamless and reproducible transformation to industrial production of nano-dispersions in flow-though mode. Hielscher sonicators are an indispensable tool for reliable micron- and nano-sized dispersions in research, analysis and industrial manufacturing.
Furthermore, doped nano-additives, e.g. as cerium oxide on MWNTs, have been successfully tested, too.
Nano-scaled, ultrasonically mono-dispersed cerium oxide offers high catalytic activity due to its high surface-to-volume ratio leading to improved fuel efficiency and reduced emissions.

Aqua-Fuels: Nano-Sized Emulsion-Fuels with Sonication

Aqua-fuels are water-in-fuel emulsions in which fine water droplets are distributed throughout a continuous fuel phase, such as diesel. Hielscher sonicators generate intense acoustic cavitation that breaks larger droplets into smaller ones, enabling the development of emulsions with nanoscale droplets under suitable formulation and processing conditions. Adjustable ultrasonic amplitude, controlled energy input, and temperature management help optimize droplet size and reproducibility, while compatible emulsifiers support stability during storage and handling.
Click here to learn more about ultrasonically prepared aqua-fuels!

 

Video: UP400St - 400 Watts Ultrasonic HomogenizerThe video shows the highly efficient emulsification of oil. The ultrasonic processor used is a Hielscher UP400St ultrasonicator, which is ideal to prepare medium size batches of high-quality emulsions.
The video shows the highly efficient emulsification of oil. The ultrasonic processor used is a Hielscher UP400St ultrasonicator, which is ideal to prepare medium size batches of high-quality emulsions.

 

Ultrasonic Fuel Blending

Ultrasonic emulsification technology is used to produce stable ethanol-in-decane, ethanol-in-diesel, or diesel–biodiesel–ethanol/bioethanol blends. Such blends are an ideal base fuel, which can be in a second step improved by dispersing nano-particles into the fuel.

Hielscher Ultrasonics supplies powerful homogenizers for the production of emulsion fuels (Click to enlarge!)

Ultrasonic production of emulsion fuels

Industrial Sonicators for Dispersing and Emulsifying Nano-Fuels

Hielscher sonicators combine effective nanoparticle deagglomeration with precise process control for nanofuel development and production. Intense ultrasonic cavitation helps break apart particle clusters and distribute additives such as metal oxides and carbon nanotubes throughout diesel, biodiesel, and blended fuels. Adjustable amplitude and monitoring of energy input and temperature support reproducible processing and formulation optimization. With laboratory instruments and industrial systems configured for batch or continuous flow-through operation, Hielscher provides a practical route from initial trials to higher production volumes. Automatic process data recording on digital industrial models helps teams document successful conditions and maintain consistent processing as throughput increases.

Scale-up and Reliable Production

Once the formulation meets its quality targets, flow-through sonication provides a route to higher production volumes. The fuel passes through an ultrasonic treatment zone at controlled operating conditions, with single-pass or recirculating processing selected according to the required result. For equipment selection, provide the base fuel, additive type and concentration, target dispersion quality, required throughput, and operating temperature. These details allow Hielscher to recommend a processor, sonotrode, and flow-cell configuration for process trials and subsequent scale-up.
Hielscher offers cost-effective, highly robust ultrasonic processors with a small footprint for the installation in plants with limited space and demanding environments.

The table below gives you an indication of the approximate processing capacity of our ultrasonicators:

Batch Volume Flow Rate Recommended Sonicator
10 to 2000mL 20 to 400mL/min UP400St
0.1 to 20L 0.2 to 4L/min UIP2000hdT
10 to 100L 2 to 10L/min UIP4000hdT
n.a. 10 to 100L/min UIP16000hdT
n.a. larger cluster of UIP16000hdT

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Produce Stable Nanofuels using Power Ultrasound!
Tell us about your fuel mixture - base fuel, nanoparticles, liquid/solid ratio and production volume. Our technical team will recommend you the best sonicator configuration and process parameters.





Ultrasonic flow-through reactor FC100L1K-1S with MultiPhaseCavitator InsertMPC48

MultiPhaseCavitator – Flow cell insert for superior nano-emulsions



Frequently Asked Questions about Ultrasonic Nanofuel Production

What are Nnano-fuels

Nano-fuels refer to a mixture of fuel and nano-particles. By the dispersing nano-energetic particles into the fuel, the physical-chemical properties of the fuel are changed by their functionlity, their dispersive structure, and the complex interplay of heat transfer, fluid flow, and particle interactions. Due to the heterogeneous composition, nanofuel characteristics are determined by the type of base fuel as well as the composition, size, shape, concentration, and physical and chemical properties of the nanoparticles. The nanofuel characteristics can differ significantly from the characteristics of the base fuel.

How is diesel used as fuel?

Diesel is liquid fuel that is burnt in diesel engines. In diesel engines, the fuel is ignited without any spark, but by compressing the inlet air mixture and then injecting the diesel fuel.
Conventional diesel fuel is a specific fractional distillate of petroleum fuel oil. In a wider sense, the term diesel refers also to fuels not derived from petroleum, e.g. biodiesel, biomass-to-liquid (BTL), gas-to-liquid (GTL), or coal-to-liquid (CTL) diesel. BTL, GTL, and CTL, are so-called synthetic diesel fuels, which can be derived from any carbonaceous material (e.g. biomass, biogas, natural gas, coal, etc.). After gasification of the raw material into synthesis gas followed by purification, it is converted via Fischer–Tropsch reaction into synthetic diesel. Ultra-low-sulfur diesel (ULSD) is a standard for diesel fuel that contains a significantly lowered sulfur content.

What is biodiesel?

Biodiesel is a renewable fuel that is produced from vegetable oils, animal fats, or recycled greases. Biodiesel can be used to run in diesel vehicles and generators. Its physical properties are similar to those of petroleum diesel, although it burns cleaner. Biodiesel reduces the emissions of unburned hydrocarbons (UHC), carbon dioxide (CO2), carbon monoxide (CO), sulfur oxides, and soot particles – when compared to emissions produced by burning conventional diesel. The emission of nitrogen oxides (NOx) can be higher for biodiesel (in comparison to diesel). However, this can be reduced by optimizing the timing of fuel injection.
Biodiesel production is greatly improved by ultrasonic transesterification. Click here to learn more about ultrasonic biodiesel production!

Can ethanol be used as fuel?

Yes, ethanol – ethyl alcohol (C₂H5OH) – can be used as fuel. Ethanol fuels are mostly used as a motor fuels – mainly as a biofuel additive in gasoline. Today, automobils can be run using 100% ethanol fuel or using so called flex-fuels, which are a blend of ethanol and gasoline. It is commonly produced by a fermentation process of biomass e.g. corn or sugarcane. Since ethanol fuel is derived from renewable, sustainable biomass, it is often called bioethanol. Power ultrasound can improve the production of bioethanol substantially. Click here to learn more about ultrasonic bioethanol production!
Ethanol is the oxygenate in E-diesel. The major drawback of E-diesel is the immiscibility of ethanol in diesel over a wide range of temperatures. However, biodiesel can be used successfully as an amphiphile surfactant to stabilize ethanol and diesel. Ethanol−biodiesel−diesel (EB-diesel) fuel can be blended ultrasonically to a micro- or nano-emulsion so that the EB-diesel is stable – even at below sub-zero temperatures and offers superior fuel properties to regular diesel fuel.

How does ultrasonic dispersion work in nanofuel production?

Ultrasonic dispersion uses acoustic cavitation to break up particle agglomerates in the fuel. Microscopic bubbles form and collapse, generating local shear forces and liquid jets that separate clustered particles. This process helps distribute nano-additives throughout the liquid and supports reproducible formulation development.

Which nanoparticles can be dispersed into fuels using ultrasound?

Materials investigated in fuel formulations include cerium oxide (CeO₂), aluminum oxide (Al₂O₃), titanium dioxide (TiO₂), zinc oxide (ZnO), and carbon nanotubes (CNTs). The appropriate additive depends on the base fuel and intended performance target. Each combination requires testing to establish suitable concentrations, processing conditions, and stability.

What is the difference between a nanofuel dispersion and a fuel nanoemulsion?

A nanoparticle dispersion contains solid particles distributed within a liquid fuel. A fuel nanoemulsion contains very small droplets of one liquid dispersed in another, such as water droplets in diesel. Ultrasound can support both processes. Formulations containing nanoparticles and dispersed liquid droplets require assessment of both particle stability and emulsion stability.

Does ultrasonic dispersion prevent nanoparticles from settling?

Ultrasonic treatment can reduce agglomeration and improve the initial distribution of particles, but lasting stability also depends on the formulation. Particle properties, additive concentration, fuel composition, and compatible dispersants influence whether particles remain suspended. Storage tests should establish how long the finished nanofuel maintains an acceptable distribution under its intended conditions.

Which ultrasonic processing parameters are most important?

Key parameters include amplitude, energy input, treatment duration, and temperature. For flow-through processing, flow rate and reactor pressure also matter. These settings should be evaluated together with the formulation. Documenting the conditions that produce the desired dispersion helps establish repeatable processing and supports subsequent scale-up.

Can ultrasonic nanofuel production be scaled from the laboratory to continuous processing?

Yes. Laboratory trials can establish the formulation and processing conditions before evaluation in an ultrasonic flow cell. In continuous operation, fuel passes through a controlled treatment zone. Scale-up should confirm that the larger system achieves the required dispersion quality and stability at the intended throughput.

How do I choose a Hielscher ultrasonic disperser for nanofuels?

Start with the base fuel, nanoparticle type and concentration, required batch volume or flow rate, and target dispersion quality. Include the operating temperature and intended storage period. These details help us to recommend the ideal sonicator, sonotrode, and flow-cell configuration for application trials and production planning.

Literature / References

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