Stable Paraffin Wax Emulsions via Sonication

Ultrasonic emulsification provides significant advantages in the preparation of stable paraffin wax emulsions, enhancing the quality and stability of the final product.
Sonication effectively overcomes the key challenges of paraffin emulsification by utilizing high-intensity ultrasonic waves to generate intense cavitation forces, which break down paraffin wax into fine droplets and ensure a uniform particle size distribution. This process enhances the stability of the emulsion by preventing phase separation and coalescence of droplets. Additionally, sonication operates efficiently at lower temperatures, reducing the risk of degrading sensitive components or causing excessive melting of the wax. The powerful ultrasonic energy facilitates the emulsification of high-viscosity wax, ensuring thorough mixing and reducing the need for excessive surfactants. This means that sonication provides a controlled and energy-efficient method to achieve stable and homogeneous paraffin wax emulsions.

Ultrasonics Paraffin Wax Emulsification

Paraffin wax emulsification is a critical process in various industries, including cosmetics, pharmaceuticals, and food production. Achieving a stable and uniform emulsion, particularly at the nanoscale, presents unique challenges. Ultrasonic emulsification is a well-established, reliable emulsification technique, applying high-intensity ultrasound waves to produce fine, stable emulsions. Probe-type sonicators and ultrasonic flow cells stand out for their efficiency and effectiveness in batch and flow-through emulsification.

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Hielscher probe-type sonicators produce stable paraffin wax nanoemulsions.

Hielscher probe-type sonicators produce stable paraffin wax nanoemulsions.

Advantages of Probe-Type Sonicators for Paraffin Wax Emulsification

Probe-type sonicators are distinguished by their ability to deliver intense ultrasonic energy directly into the medium, ensuring efficient acoustic cavitation and shear forces. This direct approach of sonication is characterized by several key benefits:

  • High Energy Efficiency: The focused application of ultrasound energy minimizes energy loss, making the process highly efficient.
  • Precision and Control: Probe-type sonicators allow precise control over the ultrasonic parameters, such as amplitude and duration, facilitating the optimization of emulsification conditions for different formulations. Tuning the sonication intensity allows to produce micro- and nano-emulsions with a very narrow droplet distribution.
  • Scalability: Probe-type sonicators are versatile, suitable for both small-scale laboratory research and large-scale industrial applications. Suitable for batch sonication or continuous flow-through sonication using an ultrasonic flow cell, makes the paraffin wax emulsion process scalable to any production level. This adaptability ensures consistent performance across different production scales.

The Role of Ultrasonic Flow Cells in Nanoemulsions

The ultrasonic flow cell is a crucial accessory when uniform processing and scalability are paramount. It integrates with probe-type sonicators to offer continuous processing capabilities. When should I use an ultrasonic flow cell?

  • Enhanced Throughput: By enabling continuous flow, the ultrasonic flow cell significantly increases processing capacity. This is particularly beneficial for industrial-scale operations where high throughput is required without compromising the quality of the emulsion.
  • Uniform Processing: The flow cell ensures that the entire volume of the emulsion is subjected to consistent ultrasonic energy, promoting uniform droplet size distribution. This is essential for the production of nanoemulsions, where droplet size uniformity directly influences stability and performance.
  • Minimized Sample Degradation: Continuous processing in a flow cell reduces the risk of overheating and degradation of sensitive components. The controlled environment within the flow cell maintains the integrity of the emulsified substances. Ultrasonic flow cells equipped with a cooling jacket for temperature control are available. Read more about temperature control during sonication!

Combining probe-type sonicators with ultrasonic flow cells represents a powerful approach to paraffin wax emulsification. This combination not only enhances the efficiency and uniformity of paraffin wax nanoemulsions and other emulsion types, but also ensures scalability and consistent quality across various applications.
 

For further information on ultrasonic paraffin wax emulsification and our range of probe-type sonicators and flow cells, please contact us now. Our well-trained team of experts in ultrasonic processing is glad to assist you!
In this short clip, we demonstrate you the quick ultrasonic emulsification of paraffin wax flakes in water. Intense ultrasound and acoustic cavitation disperse the paraffin as minute droplets in the water phase.

Ultrasonic Paraffin Emulsion - Ultrasonic Probe UP400St

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Why Hielscher Ultrasonics?

  • high efficiency
  • state-of-the-art technology
  • reliability & robustness
  • adjustable, precise process control
  • batch & inline
  • for any volume
  • intelligent software
  • smart features (e.g., programmable, data protocolling, remote control)
  • easy and safe to operate
  • low maintenance
  • CIP (clean-in-place)

Design, Manufacturing and Consulting – Quality Made in Germany

Ultrasonic emulsification is used to produce paraffin wax nanoemulsions at any production scale. The picture shows a probe-type sonicator with glass flow cell for the inline emulsification of paraffin wax.Hielscher ultrasonicators are well-known for their highest quality and design standards. Robustness and easy operation allow the smooth integration of our ultrasonicators into industrial facilities. Rough conditions and demanding environments are easily handled by Hielscher ultrasonicators.

Hielscher Ultrasonics is an ISO certified company and put special emphasis on high-performance ultrasonicators featuring state-of-the-art technology and user-friendliness. Of course, Hielscher ultrasonicators are CE compliant and meet the requirements of UL, CSA and RoHs.

The table below gives you an indication of the approximate processing capacity of our ultrasonicators:

Batch VolumeFlow RateRecommended Devices
1 to 500mL10 to 200mL/minUP100H
10 to 2000mL20 to 400mL/minUP200Ht, UP400St
0.1 to 20L0.2 to 4L/minUIP2000hdT
10 to 100L2 to 10L/minUIP4000hdT
15 to 150L3 to 15L/minUIP6000hdT
15 to 150L3 to 15L/minUIP6000hdT
n.a.10 to 100L/minUIP16000
n.a.largercluster of UIP16000

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Ultrasonic high-shear homogenizers are used in lab, bench-top, pilot and industrial processing.

Hielscher Ultrasonics manufactures high-performance ultrasonic homogenizers for mixing applications, dispersion, emulsification and extraction on lab, pilot and industrial scale.



Literature / References

Facts Worth Knowing

What is Paraffin Wax?

Paraffin wax is a white or colorless soft solid derived from petroleum, coal, or shale oil. It consists of a mixture of hydrocarbon molecules containing between twenty and forty carbon atoms. Paraffin wax is commonly used in candle making, as a lubricant, for coating and sealing purposes, and in beauty treatments. It is known for its ability to burn cleanly and its smooth, malleable texture.

What are Paraffin Wax Emulsions used for?

Paraffin wax emulsions are used in various industries. Due to characteristics such as being water-repelling, glossy, thickening, biodegradable, and stabilizing, paraffin wax emulsions fulfill a wide range of applications in industrial and consumer products. Below we list a few common industries, which utilize specific material properties of paraffin wax emulsion for improved products:

  1. Paper and Packaging Industry: Paraffin wax emulsions are used to coat paper and cardboard, providing water resistance and a glossy finish. They are also used in the production of waxed paper for food packaging.
  2. Textiles: In the textile industry, paraffin wax emulsions are used to provide water repellency and to improve the texture and feel of fabrics.
  3. Cosmetics and Personal Care: Paraffin wax emulsions are used in lotions, creams, and ointments to provide moisturizing properties and improve texture. They are also used in hair removal products like depilatory waxes.
  4. Polishes and Cleaners: These emulsions are used in floor polishes, car waxes, and furniture polishes to provide a protective and shiny coating.
  5. Agriculture: Paraffin wax emulsions are used as coatings for fruits and vegetables to extend shelf life by reducing water loss and providing a glossy appearance.
  6. Construction: In construction, paraffin wax emulsions are used as curing compounds for concrete, helping to retain moisture during the curing process and improving the strength and durability of the concrete.
  7. Lubricants: They are used as lubricants in various industrial applications where a clean and non-staining lubricant is required.

High performance ultrasonics! The Hielscher product range covers the full spectrum from the compact lab ultrasonicator over bench-top units to full-industrial ultrasonic systems.

Hielscher Ultrasonics manufactures high-performance ultrasonic homogenizers from lab to industrial size.

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