Ultrasonic Extraction of Sugar from Sugar Beet Cossettes

Ultrasonic extraction enhances the yield of extracted sucrose from sugar beet cossettes and reduces the extraction process duration significantly. Sonication is a simple and safe technique, which can be easily combined with the current counter-current flow extraction technology in order to improve extraction efficiency.

Ultrasonic Sugar Beet Cossette Extraction

The production of sucrose, also known as table sugar, can be intensified by ultrasonic extractionUltrasound-assisted extraction is based on the working principle of acoustic or ultrasonic cavitation. The mechanical effects, which are generated by ultrasonically induced cavitation, cause sono-poration and disruption of cell walls, which subsequently increases the permeability of molecules entrapped in the cell interior. Cavitationally caused liquid streaming and micro-turbulences improve the mass transfer of the extraction process, so that sucrose and other molecules are transferred into the solvent, i.e. water.

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Power ultrasound improves the extraction efficiency of sugar from sugar beet cossette. Hielscher Ultrasonics supplies high-performance ultrasonic extractors for large sugar production plants.

Ultrasonicator UIP4000hdT for industrial sugar beet extraction.

Ultrasonic extraction can be installed at various steps during sucrose extraction:

  • Ultrasonic pre-treatment (before counter-current tower)
  • Sonication during countercurrent extraction
  • Ultrasonic post-treatment (after counter-current tower)

Depending on the existing extraction facility, production targets and available space, sonication can be easily retro-fitted as pre- or post-treatment as well as during countercurrent flow extraction.

Ultrasonic Pre-Treatment of Sugar Beet Cossettes

Ultrasonic pre-treatment of sugar beet cossettes is a process intensifying technique. Ultrasonic extractors can be easily combined with counter-current flow extraction towers, which are mainly used for sugar beet extraction. A short sonication of the sugar beet cossettes before they enter the counter-current extraction system help to disrupt and open the cell walls. Ultrasonication promotes mass transfer between the solvent (i.e., water) and beet cossettes, so that the intracellular molecules such as sucrose are transferred from the cell interior to the solvent. The ultrasonic pre-treatment of sugar beet cossettes facilitates and accelerates the sucrose extraction in the counter-current flow column.

Ultrasonic extraction effects on sugar beet cossettes.

SEM (200×) of sugar beet cossette samples sonicated at 400 W at 50°C for different extraction time. A) countercurrent flow of cossettes extraction; B) after UAE for 10 min; C) after UAE for 20 min; D) after UAE for 40 min. Ultrasonic extraction disrupts the cell walls and releases the intracellular material.
(©Lu et al., 2013)

Comparison of Ultrasonic vs Counter-Current Extraction

Fuら(2013)は、従来の向流流抽出とテンサイコゼットからのショ糖の超音波抽出を比較しました。研究の結果は、超音波処理が優れた純度のより高い収率をもたらし、抽出時間が70分(向流)から40分(超音波処理)に有意に短縮されたことを示した。超音波支援抽出(UAE)は、コロイド状不純物濃度(特にペクチン)が低くなり、ショ糖収率が高くなります(94.0±0.15%)。高純度(92.6±0.11%)の抽出果汁です。(Fu et al., 2013参照)
Since sugar production facilities are already equipped with conventional countercurrent extraction towers, the combination of synergistic sonication with the existing installation is generally favoured. In order to apply ultrasonic sucrose extraction in the most cost- and time-efficient manner, ultrasonic extraction can be installed as synergistic treatment before, during, or after conventional counter-current flow extraction. As sonication disrupts the sugar beet cells and releases the sucrose from the cells, the duration of the counter-current flow treatment can be reduced, whilst the sucrose yield is enhanced.

Advantages of Ultrasonic Sucrose Extraction

  • Accelerated process
  • より高い収量
  • プロセスの強化
  • Synergetic effects w/ countercurrent systems
  • 簡単な後付け
  • Simple testing
  • 線形スケーラビリティ
  • 低メンテナンス
  • 迅速なROI

高性能超音波抽出器

Hielscher Ultrasonics’ extraction systems are used worldwide in food and pharma for the commercial production of high quality extracts used as food products, dietary supplements or pharmaceuticals. Wether you want to test and optimise ultrasonic processing parameters on bench-top level or install a fully-industrial ultrasonic extraction system for inline production, Hielscher Ultrasonics has the suitable ultrasonic extraction setup for you. A small foot print and flexible installation options allow for retro-fitting even in a crammed processing facility.

ヒールシャー超音波によるプロセス標準化

食品グレードの製品は、適正製造基準(GMP)に準拠し、標準化された処理仕様に基づいて製造する必要があります。ヒールシャー超音波のデジタル抽出システムにはインテリジェントなソフトウェアが付属しており、超音波処理プロセスを正確に設定および制御することが容易になります。自動データ記録は、超音波エネルギー(総エネルギーと正味エネルギー)、振幅、温度、圧力(温度センサーと圧力センサーが取り付けられている場合)などのすべての超音波プロセスパラメータを、内蔵SDカードに日付と時刻のスタンプで書き込みます。これにより、超音波処理された各ロットを修正できます。同時に、再現性と継続的な高い製品品質が保証されます。
Hielscher Ultrasonics’ 産業用超音波プロセッサは、非常に高い振幅を提供できます。最大200μmの振幅は、24/7動作で簡単に連続運転できます。さらに高い振幅のために、カスタマイズされた超音波ソノトロードが利用可能です。ヒールシャーの超音波装置の堅牢性は、ヘビーデューティと要求の厳しい環境での24 / 7操作を可能にします。
以下の表は、超音波装置のおおよその処理能力を示しています。

バッチボリューム流量推奨デバイス
1〜500mL10〜200mL/分UP100Hシリーズ
10〜2000mL20〜400mL/minUP200HT, UP400セント
0.1〜20L0.2〜4L / minUIP2000hdT
10〜100L2〜10L/minUIP4000hdt
N.A.さん10〜100L/minUIP16000
N.A.さん大きいクラスタ UIP16000

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ヒールシャー超音波は、分散、乳化および細胞抽出用の高性能超音波ホモジナイザーを製造しています。

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知っておく価値のある事実

Sugar Production

Sugar beets are the raw material for sucrose production. Ultrasonic extraction enhances sugar yield and accelerates the extraction time significantly. Overall, ultrasonic sugar beet cossette extraction resultins in a higher extraction efficiency. Sucrose, also known as table sugar, is mainly produced from sugar cane and from sugar beets (Beta vulgaris). Sugar, i.e., sucrose, is extracted from beets using hot water in a multi-step step process, where raw sugar juice is extracted in a hot water diffusion in a countercurrent flow system. Afterwards, the sugar juice is concentrated under vacuum, followed by cyclic washing and finally drying.

After harvest, the beet roots are transported to the sugar processing plant, where the beets are washed and then mechanically cut into thinly sliced strips, the so-called cossettes. The cossettes are fed into to counter-current flow extraction system. The countercurrent system works by diffusion and leaches the sugar content from the cossettes into hot water.
The countercurrent diffusion systems are long reactors or high towers / columns of several metres in which the cossettes flow in one direction (upwards) while hot water flows in the opposite direction (downstream). Modern tower extraction plants have a processing capacity of up to 17,000 metric tons per day. The typical retention time of cossettes in the countercurrent tower is approx. 90 min., whilst the water remains only 45 min. in the diffuser column. The main advantage of counter-current flow systems is the reduced water use when compared to sugar beet maceration in a hot water reactor. The sugar juice solution which is produced in the counter-current diffusion system is called raw juice. The raw juice colour can vary between black to dark red depending on its oxidation level.
使用済みのコゼットは、約95%の水分を持つパルプとして拡散システムから出ますが、ショ糖含有量は低くなります。
湿ったパルプをスクリュープレスで約75%の水分までプレスし、パルプから残っているスクロースを回収します。
The remaining pulp is dried and used mainly as animal feed.
Carbonatation is applied to remove impurities from raw juice before it can be precipitated to sugar crystals. Therefore, the raw juice is mixed with hot milk of lime, i.e., a suspension of calcium hydroxide in water. During the carbonatation, impurities such as sulfates, phosphates, citrate and oxalates precipitate. They precipitate in form of calcium salts and larger organic molecules , e.g. proteins, pectins, and saponins. Additionally, the alkaline pH value converts the simple sugars glucose and fructose along with the amino acid glutamine, to chemically stable carboxylic acids, which can be removed later via filtration, since those molecules would interfere with the crystallization.
In the following process step, carbon dioxide is bubbled through the alkaline sugar solution, precipitating the lime as calcium carbonate. The calcium carbonate particles bind some impurities. The heavy particles settle in the tank and can be removed via filtration.After these purification and cleaning steps the so-called thin juice is obtained. The thin juice might be treated with soda ash to adjust the pH value as well as with a sulfur-based compound to reduce colouring, which might occur due to thermal decomposition of monosaccharides.
蒸発は、多重効果蒸発システムを使用して薄いジュースを濃縮するために使用され、薄いジュースが濃厚なジュースに変わります。濃厚な果汁は、スクロースが重量で約60%含まれています。
In the final step, the thick juice is treated in crystallizers. By adding and dissolving recycled sugar, a so-called mother liquor is produced. The mother liquor is concentrated further by boiling under a vacuum in large vessels, known as vacuum pans, and very fine sugar crystal are added as seeding points. These crystals grow as sugar from the mother liquor forms around them. The resulting sugar crystal / syrup mixture is called a massecuite, a French term wich meanscooked mass. The massecuite is fed into a centrifuge, where the “High Green syrup” is removed from the massecuite by centrifugal force. After a centrifucagtion, water is then sprayed into the centrifuge to wash the sugar crystals, which produces a so-called “Low Green syrup”. The centrifuge then spins at very high speeds to partially dry the crystals. When the centrifuge slows down, the sugar is scraped from centrifuge walls onto a conveyer system to transport the sugar into a rotation granulator where it is dried by warm air. The dry, clean sugar crystals are ready to be sold to refineries or food manufacturers for further treatment or use.

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